Friday 11 May 2018

Pharmaceutical Drug Analysis - Lecture Notes, Study Materials and Important questions answers



Pharmaceutical Drug Analysis
- Lecture Notes, Study Materials and Important questions answers




Subject : Pharmaceutical Drug Analysis

GENERAL ASPECTS

Pharmaceutical Chemicals Purity and Management

  1. Pharmaceutical Chemicals: Purity and Management - Answer (click here)
  2. Pharmaceutical Chemicals: Purity - Answer (click here)
  3. Pharmaceutical Chemicals: Management - Answer (click here)
  4. Description of the Drug or Finished Product - Pharmaceutical Chemicals: Management - Answer (click here)
  5. Sampling Procedures and Errors - Pharmaceutical Chemicals: Management - Answer (click here)
  6. Bioavailability - Pharmaceutical Chemicals: Management - Answer (click here)
  7. Identification Tests - Pharmaceutical Chemicals: Management - Answer (click here)
  8. Physical Constants - Pharmaceutical Chemicals: Management - Answer (click here)
  9. Limit Tests Vis-A-Vis Quantitative Determinations - Answer (click here)
  10. Various Types of Tests for Quantitative Determinations - Pharmaceutical Chemicals: Management - Answer (click here)
  11. Limit Tests for Metallic Impurities - Answer (click here)
  12. Limit Tests for Lead - Answer (click here)
  13. Limit Test for Arsenic - Answer (click here)
  14. Limit Test’s for Acid Radical Impurities - Answer (click here)
  15. Limit Tests for Non-Metallic Impurities - Answer (click here)

Theory and Technique of Quantitative Analysis

  1. Theory and Technique of Quantitative Analysis - Answer (click here)
  2. Volumetric Analysis - Answer (click here)
  3. Volumetric Apparatus - Answer (click here)
  4. Volumetric Analysis: General Cosiderations - Answer (click here)
  5. Technique of Volumetric Analysis - Answer (click here)
  6. Biomedical Analytical Chemistry - Answer (click here)
  7. Biomedical Analytical Chemistry: Colorimetric Assays - Answer (click here)
  8. Biomedical Analytical Chemistry: Enzymatic Assays - Answer (click here)
  9. Radioimmunoassays (RIAS) - Answer (click here)
  10. Automated Methods of Clinical Analysis - Answer (click here)

Errors In Pharmaceutical Analysis and Statistical Validation

  1. Errors in Pharmaceutical Analysis - Answer (click here)
  2. Classification of Errors in Pharmaceutical Analysis - Answer (click here)
  3. Pharmaceutical Statistical Validation - Answer (click here)
  4. Statistical Treatment of Finite Samples - Answer (click here)
  5. Distribution of Random Numbers - Answer (click here)
  6. Significant Figures - Answer (click here)
  7. Comparison of Results - Answer (click here)
  8. Method of Least Squares - Answer (click here)
  9. Recommendations for Criteria of Rejecting an Observation - Answer (click here)
  10. Sampling Statistics - Answer (click here)

CHEMICAL METHODS

Aqueous Titrations

  1. Aqueous Titrations - Answer (click here)
  2. Theory of Acidimetry - Answer (click here)
  3. Aqueous Titrations: Assay of Drugs - Answer (click here)
  4. Theory of Alkalimetry - Answer (click here)

Non Aqueous Titrations

  1. Non-Aqueous Titrations - Answer (click here)
  2. Non-Aqueous Titrations: Theory - Answer (click here)
  3. Non-Aqueous Titrations: Methodology - Answer (click here)
  4. Assay by Non-Aqueous Titrations - Answer (click here)
  5. Acidimetry in Non-Aqueous Titrations - Answer (click here)
  6. Alkalimetry in Non-Aqueous Titrations - Answer (click here)

Permanganate Dichromate and Ceric Sulphate Titration Methods

  1. Permanganate, Dichromate and Ceric Sulphate Titration Methods - Answer (click here)
  2. Theory - Permanganate, Dichromate and Ceric Sulphate Titration Methods - Answer (click here)
  3. Assay Methods - Permanganate, Dichromate and Ceric Sulphate Titration Methods - Answer (click here)
  4. Permanganate Titration Methods - Answer (click here)
  5. Dichromate Titration Methods - Answer (click here)
  6. Ceric Sulphate Titration Methods - Answer (click here)

Iodimetric and Iodometric Titrations

  1. Iodimetric and Iodometric Titrations - Answer (click here)
  2. Theory - Iodimetric and Iodometric Titrations - Answer (click here)
  3. Assay Methods - Iodimetric and Iodometric Titrations - Answer (click here)
  4. Iodimetric Assays - Answer (click here)
  5. Iodometric Assays - Answer (click here)
  6. Argentometric Precipitation Methods - Answer (click here)
  7. Argentometric Precipitation Methods: Theory - Answer (click here)
  8. Argentometric Precipitation Methods: Assay Methods - Answer (click here)

Complexometric Analysis

  1. Complexometric Analysis - Answer (click here)
  2. Complexometric Analysis: Theory - Answer (click here)
  3. Complexometric Analysis: Assay Methods - Answer (click here)

Gravimetric Analysis

  1. Gravimetric Analysis - Answer (click here)
  2. Gravimetric Analysis: Theory - Answer (click here)
  3. Gravimetric Analysis: Assay Methods - Answer (click here)
  4. Substances Assayed Gravimetrically - Answer (click here)
  5. Substances Assayed After Conversion - Gravimetric Analysis - Answer (click here)

Thermoanalytical Analysis

  1. Thermoanalytical Analysis - Answer (click here)
  2. Thermogravimetric Analysis (TGA) - Answer (click here)
  3. Differential Thermal Analysis (DTA) - Answer (click here)
  4. Thermometric Titrations (TT) - Answer (click here)

Diazotization Sodium Nitrite Titration

  1. Diazotization (Sodium Nitrite Titration) - Answer (click here)
  2. Diazotization (Sodium Nitrite Titration): Assay Methods - Answer (click here)

Estimation of Phenols and Related Compounds

  1. Estimation of Phenols and Related Compounds - Answer (click here)
  2. Estimation of Phenols and Related Compounds: Assay Methods - Answer (click here)

Karl Fischer Method for Determination of Water

  1. Karl Fischer Method for Determination of Water - Answer (click here)
  2. Instrumentation - Karl Fischer Method for Determination of Water - Answer (click here)
  3. Applications of Karl Fischer Method for Determination of Water in Pharmaceutical Analysis - Answer (click here)

Tetrazolium Assay of Steroids

  1. Tetrazolium Assay of Steroids - Answer (click here)
  2. Tetrazolium Assay of Steroids: Theory - Answer (click here)
  3. Assay of Pharmaceutical Substances - Tetrazolium Assay of Steroids - Answer (click here)

ELECTROCHEMICAL METHODS

Potentiometric Methods

  1. Potentiometric Methods - Answer (click here)
  2. Potentiometric Methods: Theory - Answer (click here)
  3. Potentiometric Methods Instrumentation: Electrodes, Automatic Titrator - Answer (click here)
  4. Applications of Potentiometric Titrations in Pharmaceutical Analysis - Answer (click here)

Amperometric Methods

  1. Amperometric Methods - Answer (click here)
  2. Amperometric Methods: Theory - Answer (click here)
  3. Amperometric Methods: Instrumentation - Answer (click here)
  4. Applications of Amperometric Titrations in Pharmaceutical Substances - Answer (click here)

OPTICAL METHODS

Refractometry

  1. Refractometry - Answer (click here)
  2. Refractometry: Theory - Answer (click here)
  3. Refractometry: Instrumentation - Answer (click here)
  4. Determination of Refractive Index of Pharmaceutical Substances - Answer (click here)
  5. Applications of Refractivity - Answer (click here)

Polarimetry

  1. Polarimetry - Answer (click here)
  2. Polarimetry: Theory - Answer (click here)
  3. Polarimetry: Instrumentation - Answer (click here)
  4. Determination of Optical Activity of Pharmaceutical Substances - Answer (click here)
  5. Nephelometry and Turbidimetry - Answer (click here)
  6. Nephelometry and Turbidimetry: Theory - Answer (click here)
  7. Instruments for Nephelometry and Turbidimetry - Answer (click here)
  8. Turbidimetric Assay of Pharmaceutical Substances - Answer (click here)
  9. Nephelometric Assay of Pharmaceutical Substances - Answer (click here)

Ultraviolet and Absorption Methods

  1. Ultraviolet and Absorption Methods - Answer (click here)
  2. Ultraviolet and Absorption Methods: Theory - Answer (click here)
  3. Ultraviolet and Absorption Methods: Instrumentation - Answer (click here)
  4. Ultraviolet and Absorption Methods: Assay Methods - Answer (click here)

Infrared Spectrophotometry

  1. Infrared Spectrophotometry - Answer (click here)
  2. Infrared Spectrophotometry: Theory - Answer (click here)
  3. Infrared Spectrophotometry: Instrumentation - Answer (click here)
  4. Applications of IR-Spectroscopy in Pharmaceutical Assays - Answer (click here)
  5. Applications of IR-Spectroscopy in Analytical Chemistry - Answer (click here)

Nuclear Magnetic Resonance Spectroscopy

  1. Nuclear Magnetic Resonance Spectroscopy - Answer (click here)
  2. Nuclear Magnetic Resonance Spectroscopy: Theory - Answer (click here)
  3. Interpretation of a NMR-Spectrum - Answer (click here)
  4. Nuclear Magnetic Resonance Spectroscopy: Instrumentation - Answer (click here)
  5. Applications of NMR-Spectroscopy in Pharmaceutical Analysis - Answer (click here)

Emission Spectroscopy

  1. Emission Spectroscopy - Answer (click here)
  2. Emission Spectroscopy: Theory - Answer (click here)
  3. Emission Spectroscopy: Instrumentation - Answer (click here)
  4. Applications of Emission Spectroscopy - Answer (click here)

Flame Spectroscopy

  1. Flame Spectroscopy - Answer (click here)
  2. Flame Spectroscopy: Theory - Answer (click here)
  3. Flame Spectroscopy: Instrumentation - Answer (click here)
  4. Applications of Flame Emission Spectroscopy in Pharmaceutical Analysis - Answer (click here)

Atomic Absorption Spectroscopy

  1. Atomic Absorption Spectroscopy - Answer (click here)
  2. Atomic Absorption Spectroscopy: Theory - Answer (click here)
  3. Atomic Absorption Spectroscopy: Instrumentation - Answer (click here)
  4. Important Aspects of Atomic Absorption Spectroscopy - Answer (click here)
  5. Application of Atomic Absorption Spectroscopy in Pharmaceutical Analysis - Answer (click here)

ASSAY METHODS BASED ON SEPARATION TECHNIEQUES

Liquid Liquid Extraction

  1. Liquid-Liquid Extraction - Answer (click here)
  2. Liquid-Liquid Extraction: Theory - Answer (click here)
  3. Factors Influencing Solvent Extraction - Answer (click here)
  4. Emulsion Problem Encountered in Extractions - Answer (click here)
  5. Assay Methods Based on Liquid-Liquid Extraction - Answer (click here)

Thin Layer Chromatography TLC

  1. Thin Layer Chromatography (TLC) - Answer (click here)
  2. Thin Layer Chromatography (TLC): Theory - Answer (click here)
  3. Preparation of Thin Layers on Plates - Thin Layer Chromatography (TLC) - Answer (click here)
  4. Choice of Adsorbents - Thin Layer Chromatography (TLC) - Answer (click here)
  5. Choice Of Solvent System in Thin Layer Chromatography (TLC) - Answer (click here)
  6. Activation of Adsorbent - Thin Layer Chromatography (TLC) - Answer (click here)
  7. Purification of Silica Gel-G Layers - Thin Layer Chromatography (TLC) - Answer (click here)
  8. Spotting of the Components - Thin Layer Chromatography (TLC) - Answer (click here)
  9. Development of Thin Layers - Thin Layer Chromatography (TLC) - Answer (click here)
  10. Special Techniques in Thin Layer Chromatography (TLC) - Answer (click here)
  11. Chemical Reactions on Thin Layer Chromatography (TLC) Plates - Answer (click here)
  12. Combination of Thin Layer Chromatography (TLC) With other Techniques - Answer (click here)
  13. Detection of Components - Thin Layer Chromatography (TLC) - Answer (click here)
  14. Evaluation of the Chromatogram - Thin Layer Chromatography (TLC) - Answer (click here)
  15. Applications of TLC in Pharmaceutical Analysis - Answer (click here)

Gas Liquid Chromatography GLC

  1. Gas Liquid Chromatography (GLC) - Answer (click here)
  2. Gas Liquid Chromatography (GLC): Theory - Answer (click here)
  3. Gas Liquid Chromatography (GLC): Instrumentation - Answer (click here)
  4. Working Techniques for Quantitative Analysis - Gas Liquid Chromatography (GLC) - Answer (click here)
  5. Applications of GLC in Pharmaceutical Analysis - Answer (click here)
  6. High Performance Liquid Chromatography (HPLC) - Answer (click here)
  7. High Performance Liquid Chromatography (HPLC): Theory - Answer (click here)
  8. Instrumentation - High Performance Liquid Chromatography (HPLC) - Answer (click here)
  9. Derivatization - High Performance Liquid Chromatography (HPLC) - Answer (click here)
  10. Applications of High Performance Liquid Chromatography (HPLC) in Pharmaceutical Analysis - Answer (click here)

Size Exclusion Chromatography

  1. Size Exclusion Chromatography - Answer (click here)
  2. Size Exclusion Chromatography: Theory - Answer (click here)
  3. Size Exclusion Chromatography: Apparatus - Answer (click here)
  4. Applications of Size Exclusion Chromatography in Pharmaceutical Analysis - Answer (click here)

MISCELLANEOUS METHODS

Radioimmunoassay

  1. Radioimmunoassay - Answer (click here)
  2. Radioimmunoassay: Theory - Answer (click here)
  3. Radioimmunoassay: Instrumentation - Answer (click here)
  4. Radioimmunoassay: Methodology of the Assay - Answer (click here)
  5. Applications of Radioimmunoassay (RIA) in Pharmaceutical Analysis - Answer (click here)
  6. Novel Applications of Radioimmunoassay(RIA)-Techniques - Answer (click here)
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